I also liked the Himura Kenshin vs. Seta Sojiro fight
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Ahem.
Ichigo Kurosaki vs. Byakuya Kuchiki.
Bow down to the awesomeness. xD
And for hilarity points, probably Ichigo vs. Kisuke Urahara. >_> Or Ichigo vs. Ururu...ha!
Luffy Gear second vs. Rob Lucci. That fight was awesome. Zoro vs. Kaku.
I'm surprised no one's mentioned Light versus L, from Death Note.
FLCL episode 6 FLClimax: Naota with the power of Atomisk vs. Haruko. Pretty much any fight in FLCL was pretty cool, but that will always be a personal favorite of mine.
Indeed *kicks self again*
I also enjoyed the Luffy vs. Crocodile and the Luffy vs. Enel fights in One Piece.
You should go ahead and kick yourself again, just for good measure. Never make that mistake again. FLCL does not deserve to be forgotten.
Yes the last episode in FLCL was one of my favorites. Naruto's and Sasukes fight was pretty good also.